The Sodium Chlorate Files: A Comprehensive Manual for preparation of chlorates and perchlorates

By Jared Ledgard

Chapter 1: Equipment; A. Lab Power supplies; B. Lab Power supplies; Alternatives; C. Lab Power Supply Accessories; D. Electrodes; a) Lead electrodes; b) Graphite; electrodes; c) Lead wire; d) Copper electrodes; e) Copper tubing as electrode; E. Equipment for making electro-cells; a) Beakers; b) Glass tubes; c) Rubber stoppers and Teflon tape; d) Glass or plastic containers; e) Filter flasks; F. Miscellaneous equipment for making electro-cells; 1. Gas pumps/vacuums; 2. Plastic tubing; 3. Hot plate/magnetic stirrer; 4. Base supports and clamps; G. Buchner Funnels and Filter Flasks; 1) Vacuum Filtration; H. Vacuum Pumps; I. Thermometers and Temperature probes; J. Concentration and evaporation; K. Volumetric Cylinders; L. Stirrers; M. Hot plates; 1. Conversion factors; 2. Chemistry Calculations; Chapter 2: Preparation of Chlorine gas; A. Chlorine, An Element from the Gods'; The preparation of chlorine gas; A. Electrolysis Techniques; 01. Preparation of chlorine gas from salt and dilute sulfuric acid; 02. Preparation of chlorine gas from salt and sodium bisulfate; 03. Preparation of chlorine gas from salt and Epsom; 04. Old fashioned and most practical method of preparation of chlorine gas; 05. Preparation of chlorine gas via electrolysis of sodium bisulfate solution; 06. Preparation of chlorine gas via electrolysis of dilute sulfuric acid; 07. Preparation of chlorine gas via electrolysis of dilute hydrochloric acid; B. Non-Electrolysis Techniques; 01. Chlorine gas from sodium chloride, manganese dioxide, and sulfuric acid; Chlorine gas from Hydrochloric acid and an oxidizer; Preparation of Chlorine from manganese dioxide, sodium bisulfate monohydrate, and sodium chloride; Sodium Hypochlorite]; Preparation of 15% sodium hypochlorite; Preparation of Sodium hypochlorite solution (5.2 or 10%); Chapter 3: Preparation of Chloric Acid; Chapter 4: Preparation of Sodium Chlorate; Preparation of Sodium chlorate solution from sodium chloride via electrolysis; Sodium chlorate from bleach (sodium hypochlorite, 5.25% or 10%); Old fashion syntheses of sodium chlorate; Preparation of sodium chlorate from calcium hydroxide and chlorine followed by sodium chloride; Chapter 5: Preparation of Potassium Chlorate; Preparation of Potassium chlorate from sodium chlorate and potassium chloride; Potassium Chlorate from Bleaching powder and Potassium Chloride; Preparation of Potassium chlorate from chlorine and potassium hydroxide; Preparation of Potassium chlorate from sodium chlorate and potassium carbonate; Preparation of Potassium chlorate from potassium chloride and calcium chlorate; Preparation of Potassium chlorate directly from potassium chloride via electrolysis; Chapter 6: Preparation of Secondary Chlorates; The general properties of the chlorates; Magnesium chlorate; Calcium chlorate; Barium chlorate; Lithium chlorate; Aluminum chlorate; Silver chlorate; Ammonium Chlorate; Chapter 7: Preparation of Perchloric acid; Perchloric acid, 70%; Preparation of 70% Perchloric Acid; Preparation of perchloric acid from hypochlorous acid and ozone; Preparation of 70% perchloric acid from barium perchlorate and conc. sulfuric acid; Chapter 8: Preparation of Sodium Perchlorate and Potassium Perchlorate; Preparation of sodium perchlorate from sodium chlorate; Preparation of sodium perchlorate from ozone gas; Preparation of Potassium perchlorate directly from potassium chlorate "thermal method"; Preparation of Potassium perchlorate; Preparation of Potassium perchlorate from potassium chlorate, Lead dioxide, and sulfuric acid; Chapter 9: Preparation of Secondary Perchlorates; Magnesium perchlorate; Calcium perchlorate; Barium perchlorate; Aluminum perchlorate; Silver perchlorate; Chapter 10: Preparation of Ammonium Perchlorate; Preparation of Ammonium perchlorate; Chapter 11: Preparation of Specialty Perchlorates; Perchloryl Fluoride; Nitrosyl Perchlorate; Nitronium Perchlorate; Hydrazine perchlorate; Hydroxylamine perchlorate; Complex Perchlorates.

• Format: Paperback
• Language: English
• ISBN: B0DCJV225N
• ISBN13: 9798335324151
• Release Date: August 2024
• Publisher: Independently published
• Length: 216 Pages
• Weight: 1.45 lbs.
• Dimensions: 11.7" x 0.5" x 8.3"