Lignocellulosic residues from agrofood wastes represent an abundant but underutilized resource for the circular economy. In Egypt and the Mediterranean region, millions of tones of date palm fronds, banana pseudo-stems, vegetable processing wastes, brewery spent grain, cotton stalks, grape and olive pruning, sugar cane bagasse, and tomato residues are burned, dumped, or left to decompose annually. This book provides a practical, standardized guide for sampling and characterizing these materials as potential feedstocks for bioplastics and other value-added products. It presents reproducible protocols for site identification, sample collection, drying, milling, and holocellulose determination, applied to eleven agrofood residues across Egypt. Each case study documents biomass source, on-site management, physical characteristics, processing metrics, and chemical composition, including holocellulose content. By establishing a common language and methodology, this guide enables researchers, engineers, and policymakers to compare results, build on each other's work, and accelerate the transition from laboratory research to industrial applications.
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